Equipments

300 MHz RMN Bruker Fourier

  • operating at 6.9 T, corresponding to the resonance frequency of 300.18 MHz for the 1H nucleus.
  • automated instrument, on-flow NMR liquid sample analysis by running IconNMR under Bruker TOPSPIN 3.2 for structure elucidation of liquid samples.
  • autosampler – 16 positions.
  • 5 mm indirect observation z-gradient inverse a dual proton/carbon probe (1H/13C) – BBI probe
  • experiments available – 1D proton and carbon together with a wide range of proton homo-nuclear, 2D and hetero-nuclear proton-carbon correlation 2D experiments. Variable temperature capability for NMR experiments (250C – 650C).

500 MHz RMN Bruker Advance Ultrashield Plus

  • operating at 11.74 T, corresponding to the resonance frequency of 500.13 MHz for the 1H nucleus.
  • automated instrument, on-flow NMR sample analysis by running IconNMR under Bruker TOPSPIN 3.2 for structure elucidation of liquid samples.
  • autosampler – 16 positions.
  • two probes are available on the solution 500MHz NMR: 5 mm indirect observation z-gradient inverse (1H/13C) – BBI probe (BB / 1H / 2H Channels; X-nuclei direct detection) and 5 mm z-gradient direct observation (1H/13C/19F)- BBFO probe (BB / 1H / 2H Channels; X-nuclei direct detection).
  • experiments available – 1D proton and carbon; proton homo-nuclear 2D and hetero-nuclear proton-carbon and proton-15N 2D correlation experiments. Multi-nuclear capabilities, including 1H, 13C, 19F, 15N, 31 Capable of low and high temperature experiments with BCU-I or Liquid N2 for low temperature (-1500C –+ 1500C).